Monday, May 17, 2010

Preparation Of Starch Solution

AIM:
To prepare starch solution.
PRINCIPLE:
Starch sol is easily obtained by mixing starch paste with hot water as it is a hydrophilic colloid.
Being electrically neutral it is quite stable.
APPARATUS:
  • 250ml beakers : 2
  • Glass rod
  • Boiling tube
  • Wire gauze
  • Tripod stand
  • Funnel ( if necessary)

CHEMICALS:

  • Soluble starch powder : 1gm
  • Distilled water( ordinary pure water may also be used)

SPECIAL PRECAUTIONS:

  • The glass apparatus must be clean.
  • Starch must be added as a fine paste & never as a powder.
  • The fine paste must be prepared with water at room temperature & not with hot water.
  • Addition in a thin stream & rigorous stirring are important.

PROCEDURE:

  • Take about 100ml water in a 250ml beaker.
  • Keep it over a wire gauze on a tripod stand for heating( with a Bunsen burner).
  • Take the starch powder in a boiling tube , add some water & make it into a loose paste by shaking well.
  • When the water in the beaker has started boiling, pour the starch paste slowly in a thin stream into the boiling water, stirring vigorously with the glass rod.
  • After adding the whole paste continue boiling for about 2 minutes.
  • Allow the starch sol in the beaker to cool....( Filter if necessary- normally a clear sol will be obtained & there will be no need to filter)..

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