Wednesday, January 13, 2010

DRC of Cenex

AIM:
To determine the DRC of Cenex(Concentrated latex.

REAGENTS:
  • 2% acetic acid solution
  • distilled water.
APPARATUS:
  • Cotton waste
  • Rubber stopper
  • Wash bottle
  • 50ml Erlenmeyer flask
  • Electronic balance
  • 250ml beaker
  • Oven
  • Glass rod
  • Measuring jar

PROCEDURE:
  • Shake the sample bottle of latex.
  • Transfer 20-25ml of above latex into 50ml Erlenmeyer flask provided with a stopper.


  • Weigh about 7-10gm latex in a 250ml beaker.

  • Note the weight. A duplicate is also done.
  • Add twice the amount of distilled water per gm of latex.


  • Add double the amount of 2% acetic acid per gm of latex with constant stirring using a glass rod till the serum gets clear.

  • When the serum gets clear, filter through whatman No:1 filter paper
  • Thickness of the coagulum is reduced to about 2mm by hand roller.
  • Collect any small particles of coagulum from the beaker & filter paper by rubbing with the main bulk.
  • Wash the coagulum with running water for atleast 6 changes of water.
  • Dry the coagulum at a temperature of 50 degree celsius in an oven for 12 hours.


  • If it is not dried uniformly, then pass the coagulum through a mixing mill. Again dry in an oven at 60 degree for1 hour.
  • Cool for a while & take the final weight.


  • From the weight of the dried film & the initial weight of latex taken, the DRC of Cenex can be calculated.




No comments:

Post a Comment